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Beilstein J. Org. Chem. 2013, 9, 2028–2032, doi:10.3762/bjoc.9.239
Graphical Abstract
Figure 1: Structure of the guaiane (−)-oxyphyllol (1).
Scheme 1: Retrosynthetic analysis for (−)-oxyphyllol (1) and structures of the guaiane sesquiterpenes (+)-ori...
Scheme 2: Attempted selective deoxygenation of diol 7. a) 1 mol % K2OsO4, NMO, acetone, water, THF, rt, 97%, ...
Scheme 3: Conversion of 4 to 1. a) 20 mol % Co(acac)2, PhSiH3, 1 atm O2, THF, 0°C, 82%, diastereomeric ratio ...